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Styrax CAS 98-85-1

Molecular Formula: C8H10O

Formula Weight: 122.16

ZSpharmac: Styrax Supplier

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Product Name: Styrax
CAS No: 98-85-1
Purity: 99%

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Basic Info

Product Name:Styrax
Other Names:DL-1-Phenethylalcohol
CAS:98-85-1
Place of Origin:Shandong, China
Brand Name:ZSpharmac
Type:Cosmetic Raw Materials
Appearance:Clear colorless Liquid
EINECS No.:202-707-1
Storage:2-8°C
Provide:Styrax MSDS;
Styrax COA

What is Styrax?

Styrax and also phenylethyl alcohol are isomers, additionally called α-phenylethyl alcohol. These two substances have different frameworks and physical and chemical buildings, as well as are additionally various in scent. Su Hanxiang is smooth like a vibrator flower, and also has a purple-like aroma, while phenylethyl alcohol is generally a rose-like fragrance.Phenylethyl alcohol naturally exists in plant essential oils such as roses, bay leaves, and sandalwood, and there is no report of Styrax existing in nature. Stella alcohol is widely used in daily chemical and cosmetic industries, dyes, medicines, preservatives and other industries.

At present, large-scale industrial production adopts organic synthesis method to use acetophenone as raw material, and hydrogenation and reduction produce α-phenylethanol. Use lithium aluminum tetrahydride, sodium borohydride or aluminum isopropoxide as a catalyst to prepare phenylethyl alcohol by hydrogenation and reduction of acetophenone, but the reaction conditions are harsh and need to be carried out in an anhydrous environment, and the reaction system is homogeneous, and the product and reduction It is difficult to separate the catalysts and catalysts, the post-processing of the products is troublesome, and it is easy to cause environmental pollution. The method of heterogeneous catalytic hydrogenation can realize the effective separation of products.

The conventional method is to use hydrogen as the hydrogen source and use supported noble metals (Pt, Ru, Pd) as the catalyst to synthesize. The selectivity of the C=O reduction reaction is low, and a large amount of by-products of benzene are brought, and the reaction conditions are relatively harsh, the catalyst is expensive, and the production cost is high. In addition, alcohols are used as hydrogen sources to prepare corresponding alcohols by hydrogenation and reduction of ketones or aldehydes. The reaction conditions are mild, and the reaction temperature is generally the boiling point of the corresponding alcohols, which can be carried out under normal pressure. The catalyst used in the reaction generally only carries out the addition reaction to the carbonyl group, and has no effect on other unsaturated groups, has high selectivity, and has no by-products after the reaction.

Styrax Property

Melting point 

19-20 °C(lit.)

Boiling point 

204 °C745 mm Hg(lit.)

density 

1.012 g/mL at 25 °C(lit.)

vapor density 

4.21 (vs air)

vapor pressure 

0.1 mm Hg ( 20 °C)

refractive index 

n20/D 1.527(lit.)

Fp 

185 °F

solubility 

Chloroform (Sparingly), Ethyl Acetate, Methanol (Sparingly)

pka

14.43±0.20(Predicted)

form 

Liquid

color 

Clear colorless

Water Solubility 

29 g/L (20 ºC)

 

 

Application of Styrax

Styrax is an essential fragrance and also great chemical intermediate, which is extensively utilized in medicine, fragrance production, cosmetics, food and also great chemical sectors because of its special physical and chemical residential or commercial properties. α-Phenylethyl alcohol has a soft, positive as well as resilient increased scent. It is extensively utilized in the scent manufacturing industry for aroma adjustment, and is made use of alike soaps, cosmetics as well as perfumes. There is an excellent need both at home and also abroad.

It is utilized in large amounts when blending bitter neroli oil and also jasmine oil, as well as is utilized as the main part of climbed scent for the synthesis of various rose oils and also essential oils. It only needs to be added in a small amount in all flower fragrance blends, high-end perfumes and lotions. Very good effect, Styrax is a type of flavor that is popular amongst people and also it is steady to alkali. It is commonly utilized in soap essence and is an important flavor for mixing all climbed scent series essences. It is utilized in clove, orange blossom, It can be made use of in big amounts in many flower scents such as ylang-ylang, hyacinth, and also lily of the valley.

Styrax also has the result of repelling mosquitoes, as well as can be used to make insect repelling and also mosquito-repelling incense. It can also be utilized in percentages in food tastes, and is commonly made use of to prepare the aroma high quality of gewurztraminer and also yellow rice red wine. It is additionally commonly utilized as one of the fragrance chemical parts. It is used to regulate the flavor of flue-cured tobacco and boost the high quality of cigarette smoking as well as scent. Additionally, phenethyl alcohol is an important drug intermediate in the synthesis of many medications. For example, in the synthesis of “ibuprofen”, a sedative drug, Styrax is an important resources. This catalytic synthesis path of the medicine is considered to be very A significant development with economic worth as well as environmental management significance.

Dehydration of Styrax

Dehydration of Styrax to styrene was carried out in an Alloy 20 activator (4.3 ml. D. x 13 m) and also catalyzed by the addition of p-toluenesulfonic acid (pTSA). The reactor was operated at 26 Ombara (6 kPa), 204 ° C and also heated by 5 lbara (5100 kPa) heavy steam using an internal exchanger. Styrax was fed into the activator at a price of Mt/h as well as pTSA (130 ppm by weight of the 1-phenylethanol feed) was injected through a sparger situated at the bottom of the reactor. The conversion of Styrax was controlled at 94% by including PTSA. The vapors were dealt with in a scrubber to stay clear of PTSA carryover and the pTSA consisting of water stream was returned to the activator. The catalyst was purged from the bottom of the activator in addition to some unwanted heavy deposits.

Preparation of Styrax

Currently known synthetic methods for preparing Styrax mainly include: microbial fermentation, organic synthesis and other main methods.

Method 1: a preparation method of Styrax, said Styrax is prepared by heterogeneous hydrogenation reaction, comprising the following steps: raw material acetophenone, solvent water and catalyst are added in the reactor, and said catalyst is supported cobalt base catalyst or supported copper-based catalyst; seal the reactor, and replace it three times with nitrogen and hydrogen respectively; provide hydrogen source, control the pressure in the reactor to be 0.50~3MPa, and the stirring speed is 500~1000 rpm, at 70 Reaction at ~120°C for 2-10 hours, one-step reaction to obtain the α-phenethyl alcohol.

Method 2: a method for preparing α-phenylethyl alcohol with a magnesia/graphene hybrid material as a catalyst, the preparation method of the magnesia/graphene hybrid material catalyst comprises the following steps:

1) Preparation of graphene oxide suspension: take graphene oxide and disperse it in distilled water, and after ultrasonication for 1-3 hours, a brown-yellow graphene oxide suspension is obtained;

2) Preparation of magnesium salt solution: dissolving magnesium salt in distilled water to obtain a clear magnesium salt solution;

3) Preparation of magnesium hydroxide/graphene oxide: Dissolve ammonium bicarbonate in distilled water to make a clear ammonium salt solution, and add it to the graphene oxide suspension prepared in step 1), then add ammonia water and mix well to obtain Brown-yellow graphene oxide ammonium salt solution mixed solution; under stirring, the magnesium salt solution obtained in step 2) is dropped into the mixed solution drop by drop to obtain brown-yellow magnesium hydroxide/graphene oxide precipitate; after standing for 24 hours , placed in a water bath at 80-90°C and stirred for 4 h, filtered while hot, washed with distilled water until the filtrate was neutral, and the filter cake was exposed to the air for 24 h to obtain a gray magnesium hydroxide/graphene oxide powder cake;

4) Preparation of magnesium oxide/graphene hybrid material: place the magnesium hydroxide/graphene oxide powder cake obtained in step 3) in a drying oven at 100 °C for 24-28 h, and then roast in the air to obtain gray magnesium oxide/graphite ene hybrid materials.

Method 3: A preparation method of Styrax, the method is: under normal pressure, acetophenone is used as raw material, alcohol is used as hydrogen source, and supported alkaline earth metal oxide is used as catalyst, at a reaction temperature of 60-130°C After reacting for 1-10 hours, after the reaction is completed, the reaction solution is processed to obtain α-phenylethanol; the alcohol is C1-C7 aliphatic alcohol or C3-C7 alicyclic alcohol; the amount of the acetophenone and likewise alcohol is in between The percentage is 1:5 -30; the supported alkaline planet steel oxide is made up of a company in addition to an alkaline world metal oxide filled on the service provider, the alkaline world steel oxide is MgO, CaO, SrO or BaO, and the provider is triggered carbon, the loading amount of the alkaline earth steel oxide is 0.5-15wt% based upon the mass of the service provider.

About Products:
If you need Styrax as a cosmetic raw material, please contact our service staff directly, we will provide you with high-quality products at the best price.
As an experienced Styrax manufacturer and supplier, ZSpharmac will provide Styrax raw materials to customers all over the world for a long time.
Over the years, the company has been adhering to the spirit of “integrity management, strict quality control, customer first”, and has won unanimous praise from domestic and foreign customers.

Company Profile and Corporate Culture

Company Profile:

ZhiShang Chemical is owned by ZhiShang Group is a professional new-type chemicals enterprise combined into research and development, production and sales .

The company’s competitive product is pharmaceutical raw materials and intermediates (especially carbohydrate derivatives Series), In recent years, the company has made a major breakthrough in food and feed additives, plant extraction, industrial chemicals industry .

The company insists on the spirit of “sincere management, strict quality control, customer as god” , get consistent high praise from customers at home and abroad.

Corporate Culture:

OUR MISSION
Help China Chemicals to benefit the happiness of human life
OUR VISSION
Become the most trusted chemical supplier in the world
OUR BUSINESS PHILOSOPHY
Striver – oriented, enrich employees, customer first, deep service, seek development
OUR VALUES
Be prepared for danger in times of peace, forge ahead actively, unity and cooperation, and be brave to fight

About Us

The production base is located in Zhangqiu chemical industry park and Tai’an high-tech chemical industry park. laboratory and workshop in strict accordance with the GMP standard and the product fit national ISO9001 and ISO2000 standards.

“Zhishang” products are exported to Europe, North and South America, the Middle East, Asia Pacific and Africa area, so as to establish a long-term and stable cooperation relationship with customer in the world.

Company Info
  • Business Type: Manufacturer
  • Product Range: Cosmetic raw materials
  • Products/Service:Cosmetic raw materials (flavors and fragrances,antioxidant products, moisturizing and hydrating, whitening agents, cosmetic additives)
  • Total Employees: 51~100
  • Capital (Million US $): 10000000RMB
  • Year Established: 2016
Production Capacity
  • No. of Production Lines : 8
  • No. of QC Staff : 5 -10 People
  • OEM Services Provided : yes
  • Factory Size (Sq.meters) : 3,000-5,000 square meters
  • Certificate: ISO9001 , CE , GMP , API , MSDS
  • Factory Location : Diao Town Industry Park, Zhangqiu City, Jinan City, Shandong Province, China.

Service

Pre-Sales Service

* Prompt reply and 24 hours online, professional team to provide best price and high quality product.

* Sample testing support.

* Every batch of products will be tested to ensureits quality.

*The packing also can be according the customers` requirment.

*Any inquiries will be replied within 24 hours.

*we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate. If your markets have any special requirements, let us know.

 

After-Sales Service

*The fact of logistics information monitoring.

* Any questions about the product can be consulted at any time.

*Product has any problem can return.

FAQ

Do you accept sample order?

We will make samples before mass production, and after sample approved, we’ll begin mass production. Doing 100% inspection during production, then do random inspection before packing.

 

HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?

You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests,we will manufacture the products according to your requests.

What’s your MOQ?

Our MOQ is 1kg. But usually we accept less quantity such as 100g on the condition that sample charge is 100% paid.

Do you supply product report?

Yes. We’ll give you product analysis report before shipping.

  Is there a discount?

Different quantity has different discount.

Shipping

1. ≤50kg, Express delivery recommended, usually called as DDU service;

2. ≤500kg, Air shipping recommended, usually called as FOB, CFR, or CIF service;

3. >500kg, sea shipping recommended, usually called as FOB, CFR, or CIF service;

4. For high value products, please select air shipping and express delivery for safe.

Get Styrax Quotation