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Zhishang Chemical

N-Lsopropylbenzylamine CAS 102-97-6

Molecular Formula: C10H15N

Formula Weight: 149.23

ZSpharmac: N-Lsopropylbenzylamine Supplement

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Product Name: N-Lsopropylbenzylamine
CAS No: 102-97-6
Purity: 99%

Basic Info

Product Name:N-Lsopropylbenzylamine
Other Names:N-Benzylisopropylamine
CAS:102-97-6
Place of Origin:Shandong, China
Brand Name:ZSpharmac
Type:Organic Chemical Raw Materials
Appearance:Yellow Liquid
EINECS No.:203-067-6
Storage:Store Below +30°C.
Provide:N-Lsopropylbenzylamine MSDS;
N-Lsopropylbenzylamine COA

What is N-Lsopropylbenzylamine?

N-Lsopropylbenzylamine is a compound.N-Lsopropylbenzylamine is a compound that turns up in the chemical literature, regularly playing an intermediary function in speculative syntheses and also applications in special all-natural remodelings. In spite of its restricted videotaped use, it is understood to have included the emphasis of the DEA as a result of its usage by immoral methamphetamine manufacturers as a diluent or substitute for methamphetamine, with numerous incidents happening in between 2007 and additionally 2008. Taped explorations. Since 2018, DEA researchers associated with the methamphetamine analysis program, which recognizes taken medication samples for specific training courses and likewise other pollutants, claimed isopropylbenzylamine just showed up “occasional”. As a result, it can be utilized as a substitute or diluent for methamphetamine, which is not apparent to the individual, although various melting points and likewise different residential properties it displays, such as softer and even much more quickly busted crystals, have actually been kept in mind, as a viable sign of its presence.In Australia it is taken into consideration a boundary controlled substance. It is vague if it is an illegal drug in any other jurisdiction. N-Lsopropylbenzylamine is not thought to have any stimulant impacts, although anecdotal records suggest it might be connected with side effects such as headaches as well as complication that are not generally related to methamphetamine itself. [citation needed] The poisoning of N-Lsopropylbenzylamine has not been examined. Various other “cutting agents” discovered to have actually been utilized with methamphetamine include the related substances methylbenzylamine as well as ethylbenzylamine, as well as dimethyl sulfone.

N-Lsopropylbenzylamine Properties:

Melting point 143°C (estimate)
Boiling point 200 °C(lit.)
density 0.892 g/mL at 25 °C(lit.)
refractive index n20/D 1.502(lit.)
Fp 190 °F
storage temp. Store below +30°C.
pka9.77±0.19(Predicted)
BRN 2638437
InChIKeyLYBKPDDZTNUNNM-UHFFFAOYSA-N
CAS DataBase Reference102-97-6(CAS DataBase Reference)

 

N-Lsopropylbenzylamine Uses

  1. N-Lsopropylbenzylamine can be made use of as an intermediate in the synthesis of substances and also as a forerunner in the production of particular medicines. Due to its similarity to methamphetamine in appearance and physical properties, it has been considered by the DEA in recent years. N-Lsopropylbenzylamine forms an amine adduct with magnesium in toluene at room temperature. Using N-Lsopropylbenzylamine as ligand, bis(cyclopentadienyl)magnesium was prepared and characterized.
  2. N-Lsopropylbenzylamine is a frequently utilized organic base and an essential basic material for organic synthesis. It is a generally made use of intermediate or medication forerunner in the pharmaceutical industry.
  3. N-Lsopropylbenzylamine is an intermediate. Rust prevention.

Preparation of N-Lsopropylbenzylamine

report one,


In a 500 mL three-necked flask equipped with a thermometer, a constant-pressure dropping funnel with a drying tube, and a magnetic stirrer, lithium aluminum hydride (4.5 g, 0.12 mol) was suspended in 150 mL of dry ice-salt bath cooled of tetrahydrofuran, stirring vigorously. The N-isopropylbenzamide was dissolved in dry tetrahydrofuran (200 ml) and transferred to a dropping funnel. When the temperature of the system drops to below -5°C, slowly drop in the tetrahydrofuran solution dissolved with N-isopropylbenzamide, and the system releases heat immediately after dropping, and bubbles are released, adjust the dropping speed to make the reaction proceed smoothly. After the tetrahydrofuran solution of N-isopropylbenzamide was dripped, the reaction system was heated to reflux, and the reaction was maintained at reflux overnight. The reaction system was placed in an ice bath to cool down, and under vigorous stirring, a saturated ammonium chloride solution was slowly added. After the saturated ammonium chloride solution was continuously added, no bubbles were generated. The insoluble issue in the system was removed, and additionally ethyl acetate was used. The filter cake was cleansed countless times as well as additionally the filtrates were integrated. The filtrate was placed in a separatory network along with the layers were separated, and also the liquid layer was cleaned up with ethyl acetate till it was no longer positive by tender loving care. The natural layers were incorporated and also dried out over anhydrous magnesium sulfate over night. After drying out, anhydrous magnesium sulfate was filtered off, and likewise the filtrate was dried out under decreased pressure.Purified by ethyl acetate/dichloromethane 3:1 system column chromatography to obtain 13.6 g of pure pale yellow liquid, yield 87%
report two,


The title compound was prepared by reductive amination using a mixture of benzylamine (3 g, 28.00 mmol), acetone (2.3 ml, 31.32 mmol), MeOH (15 ml) and acetic acid (catalyst) to give N-benzyl as a colorless oil isopropylamine (1.8 g, 43.06%). 1H-NMR (500 MHz, CDCl3): δ 1.10 (d, J=6.5 Hz, 6H), 2.92 (Sep, J=6.5 Hz, 1H), 3.75 (s, 2H), 7.22 (m, 5H).

Company Profile and Corporate Culture

Company Profile:

ZhiShang Chemical is owned by ZhiShang Group is a professional new-type chemicals enterprise combined into research and development, production and sales .

The company’s competitive product is pharmaceutical raw materials and intermediates (especially carbohydrate derivatives Series), In recent years, the company has made a major breakthrough in food and feed additives, plant extraction, industrial chemicals industry .

The company insists on the spirit of “sincere management, strict quality control, customer as god” , get consistent high praise from customers at home and abroad.

Corporate Culture:

Our Mission
Help China Chemicals to benefit the happiness of human life
Our Vission
Become the most trusted chemical supplier in the world
Our Business Philosophy
Striver – oriented, enrich employees, customer first, deep service, seek development
Our Values
Be prepared for danger in times of peace, forge ahead actively, unity and cooperation, and be brave to fight

About Us

The production base is located in Zhangqiu chemical industry park and Tai’an high-tech chemical industry park. laboratory and workshop in strict accordance with the GMP standard and the product fit national ISO9001 and ISO2000 standards.

“Zhishang” products are exported to Europe, North and South America, the Middle East, Asia Pacific and Africa area, so as to establish a long-term and stable cooperation relationship with customer in the world.

Company Info
  • Business Type: Manufacturer
  • Product Range: Additive , Chemical Auxiliary & Catalyst , Organic Chemicals
  • Products/Service: Organic Intermediate,Inorganic Chemistry, APIs, Dyestuffs And Pigments, Fragrance And Spices, Food Additives
  • Total Employees: 51~100
  • Capital (Million US $): 10000000RMB
  • Year Established: 2016
Production Capacity
  • No. of Production Lines : 8
  • No. of QC Staff : 5 -10 People
  • OEM Services Provided : yes
  • Factory Size (Sq.meters) : 3,000-5,000 square meters
  • Certificate: ISO9001 , CE , GMP , API , MSDS
  • Factory Location : Diao Town Industry Park, Zhangqiu City, Jinan City, Shandong Province, China.

Service

Pre-Sales Service

* Prompt reply and 24 hours online, professional team to provide best price and high quality product.

* Sample testing support.

* Every batch of products will be tested to ensureits quality.

*The packing also can be according the customers` requirment.

*Any inquiries will be replied within 24 hours.

*we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate. If your markets have any special requirements, let us know.

 

After-Sales Service

*The fact of logistics information monitoring.

* Any questions about the product can be consulted at any time.

*Product has any problem can return.

FAQ

Do you accept sample order?

We will make samples before mass production, and after sample approved, we’ll begin mass production. Doing 100% inspection during production, then do random inspection before packing.

 

HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?

You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests,we will manufacture the products according to your requests.

What’s your MOQ?

Our MOQ is 1kg. But usually we accept less quantity such as 100g on the condition that sample charge is 100% paid.

Do you supply product report?

Yes. We’ll give you product analysis report before shipping.

  Is there a discount?

Different quantity has different discount.

Shipping

1. ≤50kg, Express delivery recommended, usually called as DDU service;

2. ≤500kg, Air shipping recommended, usually called as FOB, CFR, or CIF service;

3. >500kg, sea shipping recommended, usually called as FOB, CFR, or CIF service;

4. For high value products, please select air shipping and express delivery for safe.

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