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Zhishang Chemical

Ethylhexyl Triazone CAS 88122-99-0

Molecular Formula: C48H66N6O6

Formula Weight: 823.07

ZSpharmac: Ethylhexyl Triazone Supplement

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Product Name: Ethylhexyl Triazone
CAS No: 88122-99-0
Purity: 99%

Basic Info

Product Name:Ethylhexyl Triazone
Other Names:UV Absorber 150
CAS:88122-99-0
Place of Origin:Shandong, China
Brand Name:ZSpharmac
Type:Organic Chemical Raw Materials
Appearance:White Powder
EINECS No.:402-070-1
Storage:Keep in Dark Place,Inert Atmosphere,Room Temperature
Provide:Ethylhexyl Triazone MSDS;
Ethylhexyl Triazone COA

What is Ethylhexyl Triazone?

Triazine ultraviolet absorber, has special absorption function to UVB (275-320 nm) band, its chemical name is 4,4′,4-(1,3,5-triazine-2,4,6- Triimino) tris(2-Ethylhexyl Triazone) tribenzoate, with high photostability and prevention of UV-B-induced immunosuppression, strong water resistance, and good affinity for skin keratin.Usually only a very small dose is required in sunscreen care products to achieve high SPF value and excellent waterproof effect.

Ethylhexyl Triazone Properties:

Melting point 128°
Boiling point 869.5±75.0 °C(Predicted)
density 1.129±0.06 g/cm3(Predicted)
Fp 307℃
storage temp. Keep in dark place,Inert atmosphere,Room temperature
pka1.22±0.10(Predicted)
form neat

 

Application of Ethylhexyl Triazinone

Ethylhexyl Triazinone A novel nano-zinc oxide particle water encapsulated by ethylhexyl triazinone and OMC has been studied. Dispersions. Sun-ZerseTM is a high-efficiency, broad-spectrum zinc oxide nanodispersion with ultrafine zinc oxide encapsulated by organic UVB absorbers OT (ethylhexyl triazinone) and OMC. High pressure homogenization technology ensures 100% encapsulation stability of ultrafine zinc oxide nanodispersion. The nano-zinc oxide particles are the core of the nanospheres in the aqueous dispersion, and the core is encapsulated by organic sunscreens and esters. Phospholipids and other emulsifiers (cationic, nonionic and amphoteric surfactants) cross each other to form a mixed film surrounded by the encapsulated ultrafine zinc oxide. The above three surfactants are embedded with each other, and the oil phase and the water phase are tightly connected, and the stability of this nanodispersion is found to be satisfactory.

In addition, there is also research and preparation of an environmentally friendly lubricating oil, which contains the following components by weight: vegetable oil 70~80%, sulfurized isobutylene 7~11%, succinic acid 6~9%, diphenylamine sulfonate Sodium 2~4%, ethylhexyl triazinone 3~4% and sodium tetraborate 2~7%. Compared with the existing technology, it has higher biodegradability and lower ecotoxicity, and has good lubricating and anti-wear properties.

Preparation of Ethylhexyl Triazinone

Patent application CN10525317A discloses a preparation process of octyltriazinone and its tautomer, which adopts a mixed solution of methanol or ethanol and water for solidification; the method can obtain solidified agglomerated products, and the operation is simple, The yield is high, but the crystals cannot be formed;

Patent Application No. 639134 discloses a tautomeric form of 2,4,6-triphenylamino-p-((carbonyl-2-ethylhexyl-1-oxy)-1,3,5-triazine ( 1) preparation method, this method focuses on the solvent that recrystallization uses; Take isooctyl p-aminobenzoate and cyanuric chloride as starting materials,

Patent application CN10525317A discloses a preparation process of octyltriazinone and its tautomer, which adopts a mixed solution of methanol or ethanol and water for solidification; the method can obtain solidified agglomerated products, and the operation is simple, The yield is high, but the crystals cannot be formed;

Patent Application No. 639134 discloses a tautomeric form of 2,4,6-triphenylamino-p-((carbonyl-2-Ethylhexyl Triazinone-1-oxy)-1,3,5-triazine ( 1) preparation method, this method focuses on the solvent that recrystallization uses; Take isooctyl p-aminobenzoate and cyanuric chloride as starting materials,respond in xylene solvent to obtain 2,4,6-triphenylamine tautomeric blend of base-p-( carbonyl-2/- ethylhexyl-1/- oxy) -1,3,5- triazine; then in one or more solvents picked from the team containing Formation in the existence of: aliphatic alcohols having 2-8 carbon atoms, aliphatic carboxylic acid alkyl esters having an overall of 3-10 carbon atoms, aromatic carboxylic acid alkyl esters having a total amount of 8-12 carbon atoms, aliphatic carbonates having an overall of 3-9 carbon atoms, nitriles having a total of 2-8 carbon atoms, dialkyl ketones having a total of 3-6 carbon atoms, and Aliphatic sulfones, wherein the solvent or combination might furthermore contain approximately 30% by weight of hydrocarbons; this method can achieve a crystalline product, however the formation procedure is complicated, lengthy, and product yields are reduced; Above two technical options, all do not connect to the preparation method of target item octyl triazinone, and the technique of its formation (solidification) has issues. SUMMARY OF THE DEVELOPMENT
The function of this creation is to aim at above issue, supply the artificial technique of ultraviolet absorber Ethylhexyl Triazinone (hereinafter referred to as: UVT-150), its resources is easy to obtain, mild response problems, three wastes are couple of, and also product pureness is high. In order to fix the above-mentioned technical troubles, the technological plan adopted in the present innovation is: an artificial method of ultraviolet absorber ethylhexyl triazinone, which takes melamine, p-chlorobenzoic acid and isooctyl alcohol as beginning resources, as well as passes through two actions. Synthesis, one-step formation to obtain the target product, It is additionally called 2,4,6-tri-anilino-( p-carbonyl-2-ethylhexyl-1-oxygen) -1,3,5- triazine, 4,4′,4″-( 1, 3,5-triazine-2,4,6- triimino) Ethylhexyl Triazinone tris( 2-ethylhexyl) ester, or UV absorber UVT-150. The synthesis consists of the complying with actions:
Action 1) Synthesis of H3TATAB
The specific action in action 1) are: very first add a solvent, a catalyst, 7K, and also melamine, mix, and also dropwise right into the p-chlorobenzoic acid liquified in the exact same solvent at area temperature level; Complete the insulation reaction 4-6h; then add water for dilution, after cooling down, suction filtration, cleaning with water to nonpartisanship, draining pipes, drying out to get white strong HJATAB. Wherein, add water to dilute after the product response as well as be cooled to suction filtration after 5 ~ 10 ℃, due to the fact that the solubility of the response product in the solvent is huge, by adding water, the solubility is lowered, and also the item is separated out. Even more, the solvent symphonious 1) is a dialkyl ketone having 3-6 carbon atoms; for example: acetone, butanone, 2-pentanone, 3-pentanone, 2-hexanone, cyclohexanone or 1, 4-dioxane. This sort of solvent is needed to have solid solubility, which can much better liquify the reaction raw materials as well as the created products, and can alter the solubility by including water to separate out the produced products, as well as can also recognize the recuperation and reuse of the solvent. Better, action 1) water consumption in the response system is: 3 ~ 5 times of melamine weight; The molar intake ratio of melamine and p-chlorobenzoic acid is 1:3.1 ~ 3.3, 3 The mol proportion of polycyanamide and catalyst is 1:1.6 ~ 2. According to the theoretical proportioning quantity of material response, embrace the proportioning that p-chlorobenzoic acid is somewhat excessive, and also the usage of driver is reasonably adjusted via the examination result, and the optimum proportioning amount is figured out. The enhancement of a standard driver can efficiently promote the formation of the reaction.

Company Profile and Corporate Culture

Company Profile:

ZhiShang Chemical is owned by ZhiShang Group is a professional new-type chemicals enterprise combined into research and development, production and sales .

The company’s competitive product is pharmaceutical raw materials and intermediates (especially carbohydrate derivatives Series), In recent years, the company has made a major breakthrough in food and feed additives, plant extraction, industrial chemicals industry .

The company insists on the spirit of “sincere management, strict quality control, customer as god” , get consistent high praise from customers at home and abroad.

Corporate Culture:

Our Mission
Help China Chemicals to benefit the happiness of human life
Our Vission
Become the most trusted chemical supplier in the world
Our Busionss Philosophy
Striver – oriented, enrich employees, customer first, deep service, seek development
Our Values
Be prepared for danger in times of peace, forge ahead actively, unity and cooperation, and be brave to fight

About Us

The production base is located in Zhangqiu chemical industry park and Tai’an high-tech chemical industry park. laboratory and workshop in strict accordance with the GMP standard and the product fit national ISO9001 and ISO2000 standards.

“Zhishang” products are exported to Europe, North and South America, the Middle East, Asia Pacific and Africa area, so as to establish a long-term and stable cooperation relationship with customer in the world.

Company Info
  • Business Type: Manufacturer
  • Product Range: Additive , Chemical Auxiliary & Catalyst , Organic Chemicals
  • Products/Service: Organic Intermediate,Inorganic Chemistry, APIs, Dyestuffs And Pigments, Fragrance And Spices, Food Additives
  • Total Employees: 51~100
  • Capital (Million US $): 10000000RMB
  • Year Established: 2016
Production Capacity
  • No. of Production Lines : 8
  • No. of QC Staff : 5 -10 People
  • OEM Services Provided : yes
  • Factory Size (Sq.meters) : 3,000-5,000 square meters
  • Certificate: ISO9001 , CE , GMP , API , MSDS
  • Factory Location : Diao Town Industry Park, Zhangqiu City, Jinan City, Shandong Province, China.

Service

Pre-Sales Service

* Prompt reply and 24 hours online, professional team to provide best price and high quality product.

* Sample testing support.

* Every batch of products will be tested to ensureits quality.

*The packing also can be according the customers` requirment.

*Any inquiries will be replied within 24 hours.

*we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate. If your markets have any special requirements, let us know.

 

After-Sales Service

*The fact of logistics information monitoring.

* Any questions about the product can be consulted at any time.

*Product has any problem can return.

FAQ

Do you accept sample order?

We will make samples before mass production, and after sample approved, we’ll begin mass production. Doing 100% inspection during production, then do random inspection before packing.

 

HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?

You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests,we will manufacture the products according to your requests.

What’s your MOQ?

Our MOQ is 1kg. But usually we accept less quantity such as 100g on the condition that sample charge is 100% paid.

Do you supply product report?

Yes. We’ll give you product analysis report before shipping.

  Is there a discount?

Different quantity has different discount.

Shipping

1. ≤50kg, Express delivery recommended, usually called as DDU service;

2. ≤500kg, Air shipping recommended, usually called as FOB, CFR, or CIF service;

3. >500kg, sea shipping recommended, usually called as FOB, CFR, or CIF service;

4. For high value products, please select air shipping and express delivery for safe.

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