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Ethyl Octanoate CAS 106-32-1

Molecular Formula: C10H20O2

Formula Weight: 172.26

ZSpharmac: Ethyl Octanoate Supplement

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Product Name: Ethyl Octanoate
CAS No: 106-32-1
Purity: 99%

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Basic Info

Product Name:Ethyl Octanoate
Other Names:Ethyl Caprylate
CAS:106-32-1
Place of Origin:Shandong, China
Brand Name:ZSpharmac
Type:Cosmetic Raw Materials
Appearance:Clear Colorless Liquid
EINECS No.:203-385-5
Storage:Store Below +30°C.
Provide:Ethyl Octanoate MSDS;
Ethyl Octanoate COA

What is Ethyl Octanoate?

Ethyl Octanoate is a colorless and transparent liquid, periodically with a yellowish color, with a pineapple-like fragrance and wonderful preference. Boiling point 208.5 ℃. Insoluble in water, yet conveniently soluble in ethanol, ether, chloroform, and almost insoluble in propylene glycol. It creates an azeotropic mix with water, with an azeotrope of 98.25 ° C as well as a web content of 18%. It is prepared by home heating octanoic acid as well as ethanol under the catalysis of a small amount of concentrated sulfuric acid. Can be utilized as a flavor agent for orange, strawberry, pineapple and other seasonings. Ethyl Octanoate is a kind of edible spice specified by GB2760-96, which is mostly used to prepare flavors such as milk, cheese, apple and pineapple fruit wine, brandy, rum and so on. It is gotten by esterification of octanoic acid and ethanol.

Ethyl Octanoate Property

Melting point 

-48–47 °C (lit.)

Boiling point 

206-208 °C (lit.)

density 

0.867 g/mL at 20 °C (lit.)

vapor pressure 

0.02 mm Hg ( 25 °C)

refractive index 

n20/D 1.417(lit.)

Fp 

167 °F

storage temp. 

Store below +30°C.

solubility 

ethanol: soluble1ml/4ml, clear, colorless (70% ethanol)

form 

Liquid

color 

Clear colorless

explosive limit

0.7%(V)

Water Solubility 

insoluble

 

Ethyl Octanoate Uses

As a sucrose derivative, fatty acid sucrose ester is a safe, non-toxic, odor-free, non-polluting polyol-type non-ionic surface with excellent performance, no side effects, no irritation, good stability, and complete biodegradability. active agent. It can effectively reduce the surface tension of water, and has excellent performance in wetting, dispersing, solubilizing, foaming, emulsifying, and detergency. At the same time, it also has insecticidal and bacteriostatic properties. Therefore, it has strong adaptability and wide application range. At present, it has been widely used in food industry, daily chemical industry, pharmaceutical industry, textile, agriculture and animal husbandry and other fields, especially as emulsifier, dispersant, foaming agent, wetting agent and cleaning agent in food industry; Cosmetics, detergents, etc. in the chemical industry.

The invention CN200910029594.8 proposes a new ultrasonic synthesis process of sucrose caprylate, and synthesizes high monoesterified caprylic acid sucrose ester in high yield. The product has good hydrophilicity and thermal stability. The technical scheme of the present invention: an ultrasonic synthesis method of sucrose caprylate, using sucrose and ethyl caprylate as raw materials, potassium carbonate as a catalyst to carry out acylation reaction, the molar ratio of sucrose and ethyl caprylate is 2-2.5:1, with Dimethyl sulfoxide was used as the reaction solvent, the substrate sucrose concentration was controlled at 1 mol/L, the reaction temperature was 70-80 °C, the catalyst accounted for 9%-13% of ethyl octanoate, and the reaction pressure was 11kPa under the condition of The ultrasonic reaction was carried out for 2h in an ultrasonic cleaner with a power of 100W and an operating frequency of 40KHz. After the reaction, most of the solvent was evaporated under reduced pressure, and the distillation residue was dissolved in a sodium chloride solution with a mass concentration of 25% and a n-butanol solution under stirring. The sodium chloride solution: n-butanol V/V=1:1 , the liquids were separated, the organic phase was washed twice with a small amount of water, dried over anhydrous Na2SO4, and the solvent was removed. After the residue was washed twice with ethyl acetate, it was vacuum-dried at 45°C to constant weight to obtain a white waxy solid with a yield of 75%. % Sucrose Caprylate. CN200910029594.8 adopts green synthesis technology to synthesize sucrose octanoate with high yield. This method not only greatly shortens the reaction time, but also has high reaction selectivity, and the content of monoester in the product reaches 92%. The HLB value of the synthesized sucrose caprylate is greater than 10, has good hydrophilicity and good thermal stability, and can exist stably below 150°C.

Preparation of Ethyl Octanoate

The esterification reaction is generally a reversible reaction. In order to improve the yield of the ester, it is necessary to separate one component from the product or to make one of the components in the reactant excess so that the reaction proceeds in a positive direction. In the prior art, the method of distillation is mostly used to steam out the water in the product, thereby improving the yield of the product. However, this method consumes a lot of heating energy, which is not conducive to energy saving. The utility model CN201320461083.5 provides a rectification device for producing Ethyl Octanoate in order to overcome the above-mentioned technical problems, which can easily remove the water in the product during the reaction process, so as to achieve the purpose of improving the yield of the product. The technical scheme for solving the above-mentioned technical problems is as follows: a rectifying device for producing Ethyl Octanoate includes a rectifying tower column body, a reboiler and a condenser, and is characterized in that a guide pipe is also provided at the outlet of the condenser. Fig. 1 is the structural representation of the utility model; Fig. 2 is the structural representation of the rectifying tower in the utility model; Among the figures: 1 is the tower body, 2 is the condenser, 3 is the reboiler, 4 is the guide pipe, 11 It is the steam outlet, 12 is the reflux liquid inlet, 13 is the spray device, 14 is the packing, 15 is the return port of the reboiler, and 16 is the material inlet.

In the technical scheme of the utility model, the rectification tower adopts a packed tower, which can fully mix the reactants, and the metal corrugated structured packing has the characteristics of small resistance, uniform gas-liquid distribution, high efficiency, large energy, and insignificant amplification effect, and has the advantages of high efficiency. , pressure drop and the advantages of large flux. The tube-and-tube heat exchanger has a relatively simple, compact and inexpensive structure, which can reduce operating costs. A guide pipe is set at the outlet of the condenser. Since the product Ethyl Octanoate is insoluble in water and its mass is lighter than water, the condensate at the outlet of the condenser is in two phases of water and oil. In order to ensure that the reaction proceeds in the positive direction, during the reaction process, the water in the product is drawn out by the guide tube, and no longer participates in the reflux reaction. Therefore, the reaction time can also be reduced, manpower and material resources can be saved, and the yield of the product Ethyl Octanoate can be improved at the same time.

Company Profile and Corporate Culture

Company Profile:

ZhiShang Chemical is owned by ZhiShang Group is a professional new-type chemicals enterprise combined into research and development, production and sales .

The company’s competitive product is pharmaceutical raw materials and intermediates (especially carbohydrate derivatives Series), In recent years, the company has made a major breakthrough in food and feed additives, plant extraction, industrial chemicals industry .

The company insists on the spirit of “sincere management, strict quality control, customer as god” , get consistent high praise from customers at home and abroad.

Corporate Culture:

OUR MISSION
Help China Chemicals to benefit the happiness of human life
OUR VISSION
Become the most trusted chemical supplier in the world
OUR BUSINESS PHILOSOPHY
Striver – oriented, enrich employees, customer first, deep service, seek development
OUR VALUES
Be prepared for danger in times of peace, forge ahead actively, unity and cooperation, and be brave to fight

About Us

The production base is located in Zhangqiu chemical industry park and Tai’an high-tech chemical industry park. laboratory and workshop in strict accordance with the GMP standard and the product fit national ISO9001 and ISO2000 standards.

“Zhishang” products are exported to Europe, North and South America, the Middle East, Asia Pacific and Africa area, so as to establish a long-term and stable cooperation relationship with customer in the world.

Company Info
  • Business Type: Manufacturer
  • Product Range: Additive , Chemical Auxiliary & Catalyst , Organic Chemicals
  • Products/Service: Organic Intermediate,Inorganic Chemistry, APIs, Dyestuffs And Pigments, Fragrance And Spices, Food Additives
  • Total Employees: 51~100
  • Capital (Million US $): 10000000RMB
  • Year Established: 2016
Production Capacity
  • No. of Production Lines : 8
  • No. of QC Staff : 5 -10 People
  • OEM Services Provided : yes
  • Factory Size (Sq.meters) : 3,000-5,000 square meters
  • Certificate: ISO9001 , CE , GMP , API , MSDS
  • Factory Location : Diao Town Industry Park, Zhangqiu City, Jinan City, Shandong Province, China.

Service

Pre-Sales Service

* Prompt reply and 24 hours online, professional team to provide best price and high quality product.

* Sample testing support.

* Every batch of products will be tested to ensureits quality.

*The packing also can be according the customers` requirment.

*Any inquiries will be replied within 24 hours.

*we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate. If your markets have any special requirements, let us know.

 

After-Sales Service

*The fact of logistics information monitoring.

* Any questions about the product can be consulted at any time.

*Product has any problem can return.

FAQ

Do you accept sample order?

We will make samples before mass production, and after sample approved, we’ll begin mass production. Doing 100% inspection during production, then do random inspection before packing.

 

HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?

You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests,we will manufacture the products according to your requests.

What’s your MOQ?

Our MOQ is 1kg. But usually we accept less quantity such as 100g on the condition that sample charge is 100% paid.

Do you supply product report?

Yes. We’ll give you product analysis report before shipping.

  Is there a discount?

Different quantity has different discount.

Shipping

1. ≤50kg, Express delivery recommended, usually called as DDU service;

2. ≤500kg, Air shipping recommended, usually called as FOB, CFR, or CIF service;

3. >500kg, sea shipping recommended, usually called as FOB, CFR, or CIF service;

4. For high value products, please select air shipping and express delivery for safe.

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