Zhishang Chemical

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Zhishang Chemical

Anisonitrile CAS 874-90-8

Molecular Formula: C8H7NO

Formula Weight: 133.15

ZSpharmac: Anisonitrile Raw Material Supplier

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Product Name: Anisonitrile
CAS No: 874-90-8
Purity: 99%

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Basic Info

Product Name:Anisonitrile
Other Names:P-ANISONITRILE
CAS:874-90-8
Place of Origin:Shandong, China
Brand Name:ZSpharmac
Type:Cosmetic Raw Materials
Appearance:White to Slightly Beige Crystalline Powder
EINECS No.:212-871-6
Storage:Room Temperature
Provide:Anisonitrile MSDS;
Anisonitrile COA

What is Anisonitrile?

4-Methoxycyanobenzene is among the primary raw materials of the newly established fluorescent whitening representative in the last few years. It has important uses and excellent financial value. The existing production methods of 4-methoxycyanobenzene include diazonium salt technique, gas phase catalytic oxidation technique, amide dehydration method, etc. Nonetheless, they all have evident problems such as high poisoning, lengthy and complex process routes, high commercial application prices, and reduced returns. shortcoming.

Anisonitrile Property

Melting point 57-59 °C(lit.)
Boiling point 256-257 °C765 mm Hg(lit.)
density 1.1475 (rough estimate)
refractive index 1.5402 (estimate)
Fp 256-257°C
storage temp. Sealed in dry,Room Temperature
solubility Chloroform, Methanol
form Crystalline Powder
color White to slightly beige
Odorat 10.00 % in dipropylene glycol. sweet floral hawthorn hay coumarin
Odor Typefloral
Water Solubility soluble

 

Anisonitrile Uses

Anisonitrile has constant efficiency and is especially suitable for producing various everyday chemical, soap and tobacco flavors. Safe for skin testing. It is an outstanding raw material for mixing lily of the valley, violet and lavender scents.

Anisonitrile Preparation

Anisonitrile stage ammonia oxidation approach has actually only been reported in the previous Soviet Union and is still in its beginning in China. This approach has the advantages of uncomplicated raw materials, high selectivity, high return of the target item mononitrile, the reaction just requires to be executed in one reactor, short procedure route, a lot less contamination and light poisoning. The results of this reaction, p-toluene formaldehyde and p-toluic acid, are likewise beneficial natural chemical sources. The growth of this procedure has massive monetary worth.

The creation exposes a synthesis method of Anisonitrile, that includes the sticking to actions: (1) Area 20 mL of paraxylene in a response kettle, warmth the reaction pot to 130-135 ° C, and include solvent DMF, energizer and cocatalyst in turn, manage the oxygen feed quantity to 900mL/min, the hydrogen gas feed quantity to 100mL/min, and react for 4-5h: (2) Cool the above feedback option to area temperature, and the transparent anemic crystals gotten are 4-methoxycyanide. Benzene, make use of DMF to clean the acquired crystals 2-3 times, and eliminate the DMF solvent by suction filtering to get 4-methoxycyanobenzene with a purity higher than 90%: today invention utilizes p-methoxytoluene in the fluid stage under common pressure The one-step method of ammonia oxidation to manufacture 4-methoxycyanobenzene has high yield, high item purity and low demands for tools. It gives a remedy for the industrial production of careful oxidation of p-methoxytoluene to manufacture 4-methoxycyanobenzene. A new, much more economical and green strategy.

Speculative operation:
( 1) Take 20 mL of paraxylene and area it in the action kettle, warmth the response pot to 130 ° C, add the solvent N,N-dimethylformamide DMF, motorist and cocatalyst subsequently, the N,N-dimethylformamide The addition amount of methylformamide DMF is 20mL, the enhancement quantity of energizer and cocatalyst are 2.0 g and 10g particularly, manage the oxygen input amount to 900mL/min, the hydrogen input amount to 100mL/min, and respond for 4 hours;

( 2) Cool the above response choice to area temperature, and the clear anemic crystals gotten are 4-methoxycyanobenzene. After washing the acquired crystals two times with DMF, remove the DMF solvent by suction filtration to acquire a purity more than 90 %Anisonitrile.

Anisonitrile stage ammonia oxidation approach has actually only been reported in the previous Soviet Union and is still in its beginning in China. This approach has the advantages of uncomplicated raw materials, high selectivity, high return of the target item mononitrile, the reaction just requires to be executed in one reactor, short procedure route, a lot less contamination and light poisoning. The results of this reaction, p-toluene formaldehyde and p-toluic acid, are likewise beneficial natural chemical sources. The growth of this procedure has massive monetary worth.

The creation exposes a synthesis method of Anisonitrile, that includes the sticking to actions: (1) Area 20 mL of paraxylene in a response kettle, warmth the reaction pot to 130-135 ° C, and include solvent DMF, energizer and cocatalyst in turn, manage the oxygen feed quantity to 900mL/min, the hydrogen gas feed quantity to 100mL/min, and react for 4-5h: (2) Cool the above feedback option to area temperature, and the transparent anemic crystals gotten are 4-methoxycyanide. Benzene, make use of DMF to clean the acquired crystals 2-3 times, and eliminate the DMF solvent by suction filtering to get 4-methoxycyanobenzene with a purity higher than 90%: today invention utilizes p-methoxytoluene in the fluid stage under common pressure The one-step method of ammonia oxidation to manufacture 4-methoxycyanobenzene has high yield, high item purity and low demands for tools. It gives a remedy for the industrial production of careful oxidation of p-methoxytoluene to manufacture 4-methoxycyanobenzene. A new, much more economical and green strategy.

Speculative operation:
( 1) Take 20 mL of paraxylene and area it in the action kettle, warmth the response pot to 130 ° C, add the solvent N,N-dimethylformamide DMF, motorist and cocatalyst subsequently, the N,N-dimethylformamide The addition amount of methylformamide DMF is 20mL, the enhancement quantity of energizer and cocatalyst are 2.0 g and 10g particularly, manage the oxygen input amount to 900mL/min, the hydrogen input amount to 100mL/min, and respond for 4 hours;

( 2) Cool the above response choice to area temperature, and the clear anemic crystals gotten are 4-methoxycyanobenzene. After washing the acquired crystals two times with DMF, remove the DMF solvent by suction filtration to acquire a purity more than 90 %Anisonitrile.

Contact Us

About Products:
If you need the cosmetic raw material Anisonitrile, please contact our service staff directly, we will provide you with high-quality products at the best price.
As an experienced Anisonitrile manufacturer and supplier, ZSpharmac will provide Anisonitrile raw materials to customers around the world for a long time.
Over the years, the company has adhered to the spirit of “integrity management, strict quality control, and customer first” and has won unanimous praise from customers at home and abroad.

Company Profile and Corporate Culture

Company Profile:

ZhiShang Chemical is owned by ZhiShang Group is a professional new-type chemicals enterprise combined into research and development, production and sales .

The company’s competitive product is pharmaceutical raw materials and intermediates (especially carbohydrate derivatives Series), In recent years, the company has made a major breakthrough in food and feed additives, plant extraction, industrial chemicals industry .

The company insists on the spirit of “sincere management, strict quality control, customer as god” , get consistent high praise from customers at home and abroad.

Corporate Culture:

OUR MISSION
Help China Chemicals to benefit the happiness of human life
OUR VISSION
Become the most trusted chemical supplier in the world
OUR BUSINESS PHILOSOPHY
Striver – oriented, enrich employees, customer first, deep service, seek development
OUR VALUES
Be prepared for danger in times of peace, forge ahead actively, unity and cooperation, and be brave to fight

About Us

The production base is located in Zhangqiu chemical industry park and Tai’an high-tech chemical industry park. laboratory and workshop in strict accordance with the GMP standard and the product fit national ISO9001 and ISO2000 standards.

“Zhishang” products are exported to Europe, North and South America, the Middle East, Asia Pacific and Africa area, so as to establish a long-term and stable cooperation relationship with customer in the world.

Company Info
  • Business Type: Manufacturer
  • Product Range: Cosmetic raw materials
  • Products/Service:Cosmetic raw materials (flavors and fragrances,antioxidant products, moisturizing and hydrating, whitening agents, cosmetic additives)
  • Total Employees: 51~100
  • Capital (Million US $): 10000000RMB
  • Year Established: 2016
Production Capacity
  • No. of Production Lines : 8
  • No. of QC Staff : 5 -10 People
  • OEM Services Provided : yes
  • Factory Size (Sq.meters) : 3,000-5,000 square meters
  • Certificate: ISO9001 , CE , GMP , API , MSDS
  • Factory Location : Diao Town Industry Park, Zhangqiu City, Jinan City, Shandong Province, China.

Service

Pre-Sales Service

* Prompt reply and 24 hours online, professional team to provide best price and high quality product.

* Sample testing support.

* Every batch of products will be tested to ensureits quality.

*The packing also can be according the customers` requirment.

*Any inquiries will be replied within 24 hours.

*we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate. If your markets have any special requirements, let us know.

 

After-Sales Service

*The fact of logistics information monitoring.

* Any questions about the product can be consulted at any time.

*Product has any problem can return.

FAQ

Do you accept sample order?

We will make samples before mass production, and after sample approved, we’ll begin mass production. Doing 100% inspection during production, then do random inspection before packing.

 

HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?

You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests,we will manufacture the products according to your requests.

What’s your MOQ?

Our MOQ is 1kg. But usually we accept less quantity such as 100g on the condition that sample charge is 100% paid.

Do you supply product report?

Yes. We’ll give you product analysis report before shipping.

  Is there a discount?

Different quantity has different discount.

Shipping

1. ≤50kg, Express delivery recommended, usually called as DDU service;

2. ≤500kg, Air shipping recommended, usually called as FOB, CFR, or CIF service;

3. >500kg, sea shipping recommended, usually called as FOB, CFR, or CIF service;

4. For high value products, please select air shipping and express delivery for safe.

Get Anisonitrile Quotation