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Zhishang Chemical

1,2-Octanediol CAS 1117-86-8

Molecular Formula: C8H18O2

Formula Weight: 146.23

ZSpharmac: 1,2-Octanediol Supplier

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Product Name: 1,2-Octanediol
CAS No: 1117-86-8
Purity: 99%

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Basic Info

Product Name:1,2-Octanediol
Other Names:1,2-Octanediol, 99%
CAS:1117-86-8
Place of Origin:Shandong, China
Brand Name:ZSpharmac
Type:Cosmetic Raw Materials
Appearance:Colorless to White Low Melting Solid
EINECS No.:214-254-7
Storage:Sealed in dry,Room Temperature
Provide:1,2-Octanediol MSDS;
1,2-Octanediol COA

What is 1,2-Octanediol?

1,2-octanediol is an anemic fluid or white strong, and also its boiling point ( ° C) under the problem of 1330Pa is 131-132 ° C. 1,2-Octanediol can be mixed with numerous organic chemicals in any proportion, as well as has good formula compatibility.

1,2-Octanediol Property

Melting point 36-38 °C (lit.)
Boiling point 131-132 °C/10 mmHg (lit.)
density 0.914
vapor density >1 (vs air)
refractive index 1.4505 (estimate)
Fp >230 °F
storage temp. Sealed in dry,Room Temperature
solubility 3 g/L (20°C)
form Low Melting Solid
pka14.60±0.10(Predicted)
color Colorless to white
Water Solubility 3 g/L (20 ºC)

 

Application of 1,2-Octanediol

CN200780041024.X reports an eyelid scrub composition containing polyhexamethylene biguanide (PHMB), 1,2-hexanediol, 1,2-octanediol, and an effective amount to present the composition The pH level of the pH stabilized surfactant solution is controlled between 5.5 and 7.5. The composition may also contain humectants and foam stabilizers. The composition can be used as an eyelid scrub in conjunction with a fabric pad, where the fabric pad is pre-moistened with the composition and packaged for use. The composition can be applied to an eyelid scrub and can be rubbed to create a lather. The composition can be prepared by preparing a modified Ringer’s solution and adding 1,2-hexanediol, 1,2-octanediol, and an effective amount of one or more pH stabilizing actives. The mixture was then heated and allowed to cool before the polyhexamethylene biguanide was added.

Preparation of 1,2-Octanediol

Report One,
To the reactor equipped with stirring, thermometer and overhead tank, add formic acid and hydrogen peroxide, start stirring, then add 1-octene, after the addition, the reaction mixture solution is kept for 100 minutes, and then the formic acid and the formic acid are evaporated under reduced pressure. Water, then add sodium hydroxide solution under stirring until the pH value of the mixture solution is alkaline, then add ester to extract, the obtained extract is washed twice with sodium chloride with a concentration of 30%, and the washed extract is added without After dehydration of magnesium sulfate water, vacuum distillation is performed, and fractions are collected under the condition of 131°C/1330Pa, and the obtained fractions are the product 1,2-octanediol. The reaction temperature in the reactor is controlled at 20-90°C.

Report Two,


1. Synthesis

In a four-necked flask, install an electric stirrer, a condenser, a thermometer, an external cold water bath, and a dropping funnel. Add metered formic acid, hydrogen peroxide and catalyst to the flask in turn, and stir vigorously to mix thoroughly. Under external cooling, add a metered amount of 1-octene dropwise, control the temperature in the bottle to react at 35°C-40°C, after the dropwise addition, keep the reaction at 40°C-45°C for 3-4 hours, and then stir at room temperature After 1-2 hours of reaction, a clear and transparent mixed solution can be obtained. The clear and transparent mixed solution was distilled under high vacuum and reduced pressure, and the water and excess formic acid were distilled off until only an oily substance remained.

2. Neutralization and extraction

In a four-necked flask, configure an electric stirrer, a thermometer, a cold water bath, a condenser, and a dropping funnel. Put the above-mentioned oily substance into the flask, turn on the stirrer, control the temperature in the flask at 40℃-45℃, add 30% NaOH solution dropwise for neutralization, and add enough NaOH solution to make the pH value of the solution rise to 12 -13. After the pH value is stable, sample and analyze, and after passing the test, neutralize the obtained mixed solution with 30% HCl at 20 °C to make the pH value of the mixed solution 7, and the neutralization time is about 3h. Add solid NaCl to the mixed solution to make the aqueous phase a saturated brine mixture. Then add an appropriate amount of ethyl acetate for extraction, and the extract is saturated with

Washed with brine, finally dried over anhydrous Na2SO4 and vacuum filtered.

3. Distillation

The filtrate was concentrated under reduced pressure, and the ethyl acetate was evaporated until only oil remained; then the oil was distilled under reduced pressure at 1.33*103Pa, and the product was evaporated, which was a colorless, transparent liquid with a pungent odor. It was analyzed by gas chromatograph FID-6890 area normalization method, and the content was more than 99%.

About Products:
If you need 1,2-Octanediol, a cosmetic raw material, please contact our service staff directly, we will provide you with high-quality products at the best price.
Our company, as an experienced 1,2-Octanediol manufacturer and supplier, ZSpharmac will provide 1,2-Octanediol raw materials to customers all over the world for a long time.
Over the years, the company has been adhering to the spirit of “integrity management, strict quality control, and customer first”, and has won unanimous praise from domestic and foreign customers.

Company Profile and Corporate Culture

Company Profile:

ZhiShang Chemical is owned by ZhiShang Group is a professional new-type chemicals enterprise combined into research and development, production and sales .

The company’s competitive product is pharmaceutical raw materials and intermediates (especially carbohydrate derivatives Series), In recent years, the company has made a major breakthrough in food and feed additives, plant extraction, industrial chemicals industry .

The company insists on the spirit of “sincere management, strict quality control, customer as god” , get consistent high praise from customers at home and abroad.

Corporate Culture:

OUR MISSION
Help China Chemicals to benefit the happiness of human life
OUR VISSION
Become the most trusted chemical supplier in the world
OUR BUSINESS PHILOSOPHY
Striver – oriented, enrich employees, customer first, deep service, seek development
OUR VALUES
Be prepared for danger in times of peace, forge ahead actively, unity and cooperation, and be brave to fight

About Us

The production base is located in Zhangqiu chemical industry park and Tai’an high-tech chemical industry park. laboratory and workshop in strict accordance with the GMP standard and the product fit national ISO9001 and ISO2000 standards.

“Zhishang” products are exported to Europe, North and South America, the Middle East, Asia Pacific and Africa area, so as to establish a long-term and stable cooperation relationship with customer in the world.

Company Info
  • Business Type: Manufacturer
  • Product Range: Cosmetic raw materials
  • Products/Service:Cosmetic raw materials (flavors and fragrances,antioxidant products, moisturizing and hydrating, whitening agents, cosmetic additives)
  • Total Employees: 51~100
  • Capital (Million US $): 10000000RMB
  • Year Established: 2016
Production Capacity
  • No. of Production Lines : 8
  • No. of QC Staff : 5 -10 People
  • OEM Services Provided : yes
  • Factory Size (Sq.meters) : 3,000-5,000 square meters
  • Certificate: ISO9001 , CE , GMP , API , MSDS
  • Factory Location : Diao Town Industry Park, Zhangqiu City, Jinan City, Shandong Province, China.

Service

Pre-Sales Service

* Prompt reply and 24 hours online, professional team to provide best price and high quality product.

* Sample testing support.

* Every batch of products will be tested to ensureits quality.

*The packing also can be according the customers` requirment.

*Any inquiries will be replied within 24 hours.

*we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate. If your markets have any special requirements, let us know.

 

After-Sales Service

*The fact of logistics information monitoring.

* Any questions about the product can be consulted at any time.

*Product has any problem can return.

FAQ

Do you accept sample order?

We will make samples before mass production, and after sample approved, we’ll begin mass production. Doing 100% inspection during production, then do random inspection before packing.

 

HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?

You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests,we will manufacture the products according to your requests.

What’s your MOQ?

Our MOQ is 1kg. But usually we accept less quantity such as 100g on the condition that sample charge is 100% paid.

Do you supply product report?

Yes. We’ll give you product analysis report before shipping.

  Is there a discount?

Different quantity has different discount.

Shipping

1. ≤50kg, Express delivery recommended, usually called as DDU service;

2. ≤500kg, Air shipping recommended, usually called as FOB, CFR, or CIF service;

3. >500kg, sea shipping recommended, usually called as FOB, CFR, or CIF service;

4. For high value products, please select air shipping and express delivery for safe.

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